Introducción a la HPLC: aplicación y práctica. Front Cover. Oscar Alberto Quattrocchi. Artes Gráficas Farro, – pages. 6 oct. We are always happy to assist you. Document Description. Introduccion a La HPLC Quattrocchi. Document Share. Documents Related. Results: the HPLC method described for the simultaneous determination of sulphadoxine and pyrimethamine in mL .. Quattrocchi OA, De Andrizzi SA, Laba RF. Introducción a la HPLC Aplicación y. Práctica. Buenos Aires: Artes Gráficas.

Author: Mazushicage Faulkree
Country: Myanmar
Language: English (Spanish)
Genre: Art
Published (Last): 26 September 2012
Pages: 79
PDF File Size: 11.76 Mb
ePub File Size: 1.30 Mb
ISBN: 968-6-76242-133-8
Downloads: 41288
Price: Free* [*Free Regsitration Required]
Uploader: Gobar

Acta59 Sample application was done quatrocchi 4 mm bands. Hashemi, Electroanalysis 24, In total there are 6 users online:: Chailapakul, Talanta 79, The solutions were protected from light with an aluminum foil wrapping and usually freshly prepared solutions were used.

Book recommendation – Chromatography Forum

Tue Aug 17, 7: Thank you guys, I’ll try to find them to buy, here in Brazil we do not have many options, only a couple of books by local authors, but they treat the basics only. No interference was observed.

Chloroform, ethyl acetate, cyclohexane and ethanol were obtained from Merck Darmstadt, Germany. The analysis is fast, and the method allows a large number of samples untroduccion be measured simultaneously. Wed Mar 07, 6: The selectivity of the method was examined by preparing and analyzing checked by analyzing human serum samples spiked with nifedipine and the internal standard carbamazepine.


The nifedipine concentration ranged between 0. Antimicrobial therapy in veterinary medicine, 2nd ed. Best luck Mucha suerte Fernando. Precision was calculated by RSD and accuracy was quatfrocchi from percentage recoveries obtained by the analysis of the quality control samples, determined by linear regression equation of peak area vs.

Introduccion a La HPLC Quattrocchi

The volume of serum used was 2 mL. Acta6 No registered users and 6 guests. The linear range was between 0. The best mobile phase was a mixture of chloroform: Wed Aug 11, 4: But, I will read this book too, thanks.

Resolution R S between both peaks was 3. Inter-assay precision and inter-assay accuracy were calculated after repeated analysis in three different analytical runs. Complete resolution of the peaks with clear baseline separation was obtained of this way.

Chile, The accuracy and precision did not exceed 4. Sat Nov 30, 8: Quatteocchi Merck veterinary manual. There is a list of some recommended books on our web site: Calibration curves were constructed using peak-area ratio for the nifedipine and the internal standard carbamazepine as a function of intriduccion concentration added.


Accordingly, a method for the determination of sulfamethazine was developed using differential pulse voltammetry, at pH 11 and with an accumulation time of 3 min. The method was applied to the determination of sulfamethazine in a veterinary commercial solution.

Introduccion a La HPLC Quattrocchi – Documents

Sulfamethazine; carbon paste; ionic liquid; modified electrodes; voltammetry. Fri Jan 19, Pharmaceutics, Later, blank serum samples were spiked with this solution, to obtain final concentrations of 0. Application of the method The nifedipine concentration ranged between 0.

Dong, Talanta 76, The chromatographic conditions were arrived at after investigating several parameters, such as detection wavelength, ideal mobile phase and their proportions, internal standards, and optimal conditions for sample extraction. Hello people, I am starting to work with chromatography and would like to recommend some books, I would like to better understand how to predict retention times according to chosen column and mobile phase and other things.